5L7H
MCR IN COMPLEX WITH ligand
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-08-31 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.972 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 48.670, 77.890, 78.620 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.270 - 1.840 |
R-factor | 0.1952 |
Rwork | 0.194 |
R-free | 0.22430 |
RMSD bond length | 0.010 |
RMSD bond angle | 0.970 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Refinement software | BUSTER (2.11.6 PACIOREK) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 48.670 |
High resolution limit [Å] | 1.840 |
Rmerge | 0.093 |
Number of reflections | 26648 |
<I/σ(I)> | 12.2 |
Completeness [%] | 100.0 |
Redundancy | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 293 | 0.9 M AMS 0.1 M CHES pH 9.5 +10% Morpheus G5 |