5L7A

The crystal structure of the Human SNF5/INI1 domain

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU FR-E+ SUPERBRIGHT
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2016-05-21
Detector	MARRESEARCH
Wavelength(s)	1.54179
Spacegroup name	P 1 21 1
Unit cell lengths	43.619, 73.653, 46.460
Unit cell angles	90.00, 106.60, 90.00

Refinement procedure

Resolution	21.419 - 2.102
R-factor	0.2026
Rwork	0.200
R-free	0.26020
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	5l7b
RMSD bond length	0.008
RMSD bond angle	0.918
Data reduction software	XDS
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	PHENIX ((dev_2386: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	45.000	2.220
High resolution limit [Å]	2.100	2.100
Rmerge	0.060	0.438
Number of reflections	15711
<I/σ(I)>	14.6
Completeness [%]	95.6
Redundancy	3.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION	7.5	277	1.4 M tri-sodium citrate and 100 mM HEPES pH 7.5