Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2006-12-03 |
| Detector | MARMOSAIC 225 mm CCD |
| Wavelength(s) | 1.007829 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 85.290, 144.420, 312.110 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 52.018 - 3.500 |
| R-factor | 0.2888 |
| Rwork | 0.287 |
| R-free | 0.32390 |
| Structure solution method | SIRAS |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.873 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | autoSHARP |
| Refinement software | PHENIX (dev_2376) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 100.000 | 3.600 | |
| High resolution limit [Å] | 3.500 | 30.000 | 3.500 |
| Rmerge | 0.154 | 0.053 | 0.849 |
| Number of reflections | 49499 | ||
| <I/σ(I)> | 8.67 | 19.08 | 1.83 |
| Completeness [%] | 99.8 | 26.4 | 99.9 |
| Redundancy | 7.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6 | 277 | PEG 400, Sucrose, KCl, C12E8, Cymal-5, DDM, MES pH 6.0 |
