5KR1

Protease PR5-DRV

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RUH3R
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2015-03-07
Detector	RIGAKU
Wavelength(s)	1.5418
Spacegroup name	P 21 21 21
Unit cell lengths	50.960, 58.000, 61.730
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.141 - 1.600
R-factor	0.1893
Rwork	0.187
R-free	0.21940
RMSD bond length	0.007
RMSD bond angle	1.155
Data reduction software	iMOSFLM (7.1.1)
Data scaling software	Aimless
Phasing software	PHASER (2.1)
Refinement software	PHENIX (1.9_1692)

Data quality characteristics

	Overall
Low resolution limit [Å]	21.800
High resolution limit [Å]	1.600
Number of reflections	24794
<I/σ(I)>	14.6
Completeness [%]	99.9
Redundancy	6.09

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		300	Ammonium sulfate