5KQ8
PANK3-AMPPN complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-11-29 |
Detector | RAYONIX MX300-HS |
Wavelength(s) | 1.0 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 98.477, 98.477, 68.495 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 42.642 - 2.002 |
R-factor | 0.1827 |
Rwork | 0.181 |
R-free | 0.21850 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5kpr |
RMSD bond length | 0.008 |
RMSD bond angle | 1.034 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.642 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.105 | 0.992 |
Number of reflections | 26151 | |
<I/σ(I)> | 24.6 | 2 |
Completeness [%] | 99.9 | 100 |
Redundancy | 8.8 | 7 |
CC(1/2) | 0.749 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 291.15 | PEG 4000, ammonium acetate, citrate |