5KAW
The structure of SAV2435 bound to TETRAPHENYLPHOSPHONIUM and RHODAMINE 6G
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-02-05 |
Detector | RIGAKU SATURN 944+ |
Wavelength(s) | 1.54 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 73.724, 73.724, 65.891 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.860 - 1.860 |
R-factor | 0.1667 |
Rwork | 0.165 |
R-free | 0.19380 |
RMSD bond length | 0.005 |
RMSD bond angle | 0.978 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 36.860 |
High resolution limit [Å] | 1.860 |
Number of reflections | 15185 |
<I/σ(I)> | 19.4 |
Completeness [%] | 96.3 |
Redundancy | 11.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293 | 2.4 M ammonium sulfate, 0.1 M Tris pH 8.5 |