5K7R

MicroED structure of trypsin at 1.7 A resolution

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	53.184, 56.428, 64.672
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	25.860 - 1.700
R-factor	0.2495
Rwork	0.248
R-free	0.28110
RMSD bond length	0.005
RMSD bond angle	0.739
Refinement software	PHENIX ((1.10_2155: ???))

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	27.630	27.630	1.530
High resolution limit [Å]	1.500	8.220	1.500
Rmerge	0.773	0.210	3.632
Rpim	0.332	0.078	3.240
Number of reflections	23542	217	281
<I/σ(I)>	2.3	7.6	0.3
Completeness [%]	73.8	94.2	18.2
Redundancy	6.2	7.4	1.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1