5K7P

MicroED structure of xylanase at 2.3 A resolution

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	48.161, 59.752, 69.812
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	25.549 - 2.300
R-factor	0.2313
Rwork	0.230
R-free	0.26700
RMSD bond length	0.002
RMSD bond angle	0.496
Refinement software	PHENIX ((1.10_2155: ???))

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	25.550	25.550	1.940
High resolution limit [Å]	1.900	8.910	1.900
Rmerge	0.428	0.122	2.477
Rpim	0.245	0.064	2.214
Number of reflections	10664	151	214
<I/σ(I)>	2.7	7.1	0.4
Completeness [%]	66.6	84.6	20.4
Redundancy	3.6	3.9	1.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1