5JTU
Crystal structure of GPb in complex with 8b
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I911-2 |
Synchrotron site | MAX II |
Beamline | I911-2 |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 2015-09-06 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.0403 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 128.620, 128.620, 116.290 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.420 - 1.850 |
R-factor | 0.17186 |
Rwork | 0.170 |
R-free | 0.20269 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.010 |
RMSD bond angle | 1.304 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | REFMAC |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.760 | 1.950 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.111 | 0.450 |
Number of reflections | 74394 | |
<I/σ(I)> | 4.9 | 2.6 |
Completeness [%] | 89.9 | 94.8 |
Redundancy | 4.4 | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | SMALL TUBES | 6.7 | 289 | 10mM BES buffer |