Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-01-28 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.97242 |
| Spacegroup name | P 1 |
| Unit cell lengths | 88.820, 95.320, 107.570 |
| Unit cell angles | 83.45, 65.75, 61.99 |
Refinement procedure
| Resolution | 49.004 - 3.004 |
| R-factor | 0.235 |
| Rwork | 0.233 |
| R-free | 0.27740 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 5d3m |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.006 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 3.080 |
| High resolution limit [Å] | 3.000 | 3.000 |
| Rmerge | 0.043 | |
| Number of reflections | 52519 | |
| <I/σ(I)> | 10.54 | |
| Completeness [%] | 92.6 | 86.6 |
| Redundancy | 1.76 | 1.72 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 278 | 50MM TRIS, 17% PEG 350MME, 2% NG, 10MM SPERMIDINE |
