5JS4
Crystal structure of phiAB6 tailspike
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSRRC BEAMLINE BL15A1 |
| Synchrotron site | NSRRC |
| Beamline | BL15A1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-11-22 |
| Detector | RAYONIX MX300HE |
| Wavelength(s) | 1.0 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 135.018, 77.980, 248.080 |
| Unit cell angles | 90.00, 100.46, 90.00 |
Refinement procedure
| Resolution | 19.980 - 1.480 |
| R-factor | 0.13655 |
| Rwork | 0.136 |
| R-free | 0.15588 |
| Structure solution method | SAD |
| RMSD bond length | 0.004 |
| RMSD bond angle | 1.062 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHENIX |
| Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 1.530 |
| High resolution limit [Å] | 1.480 | 1.480 |
| Rmerge | 0.054 | 0.606 |
| Number of reflections | 406268 | |
| <I/σ(I)> | 34.3 | 3.3 |
| Completeness [%] | 96.6 | 95.3 |
| Redundancy | 7 | 7.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 1.0M sodium malonate |
