5JOQ
Crystal Structure of an ABC Transporter Substrate-Binding Protein from Listeria monocytogenes EGD-e
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-G |
Synchrotron site | APS |
Beamline | 21-ID-G |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-02-17 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 0.97857 |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 118.380, 118.380, 106.000 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 33.410 - 1.990 |
R-factor | 0.152 |
Rwork | 0.151 |
R-free | 0.17100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2q8q |
RMSD bond length | 0.014 |
RMSD bond angle | 1.002 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | MOLREP |
Refinement software | PHENIX ((DEV_2203)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 33.410 | 2.040 |
High resolution limit [Å] | 1.990 | 1.990 |
Rmerge | 0.091 | 0.662 |
Number of reflections | 30557 | |
<I/σ(I)> | 21.7 | 4.3 |
Completeness [%] | 99.9 | 99.7 |
Redundancy | 12 | 11.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 2M NH4 Citrate pH 7, 0.1M Bis-Tris Propane pH 7 |