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5JFY

Crystal structure of a plant cytidine deaminase

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsCLSI BEAMLINE 08ID-1
Synchrotron siteCLSI
Beamline08ID-1
Temperature [K]100
Detector technologyCCD
Collection date2015-06-20
DetectorRAYONIX MX300HE
Wavelength(s)0.97949
Spacegroup nameP 43 21 2
Unit cell lengths99.808, 99.808, 143.061
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution44.635 - 2.101
R-factor0.1822
Rwork0.181
R-free0.21360
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2b3j
RMSD bond length0.003
RMSD bond angle0.500
Data reduction softwareXDS
Data scaling softwareAimless
Phasing softwarePHASER (2.6.0)
Refinement softwarePHENIX
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]47.67047.6702.160
High resolution limit [Å]2.1008.9102.100
Rmerge0.0800.0200.607
Total number of observations10143113386639
Number of reflections41687
<I/σ(I)>9.738.91.4
Completeness [%]97.984.995
Redundancy2.42.52
CC(1/2)0.9970.9990.622
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP4.6293.150.0085 M CoCl2, 0.085 sodium acetate pH 4.6, 0.85 M 1,6-hexanediol, 15% (v/v) glycerol

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