5JFK

Crystal structure of a TDR receptor

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 22-ID
Synchrotron site	APS
Beamline	22-ID
Temperature [K]	100
Detector technology	CCD
Collection date	2015-04-23
Detector	RAYONIX MX300-HS
Wavelength(s)	1.0422
Spacegroup name	P 41
Unit cell lengths	92.336, 92.336, 250.127
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	46.168 - 2.647
R-factor	0.2226
Rwork	0.222
R-free	0.24970
RMSD bond length	0.005
RMSD bond angle	1.102
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX (1.9_1692)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.647
Number of reflections	56517
<I/σ(I)>	17.2
Completeness [%]	93.1
Redundancy	3.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	EVAPORATION		298	200mM MgSO4, 20% PEG3350