5JFI

Crystal structure of a TDIF-TDR complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 22-ID
Synchrotron site	APS
Beamline	22-ID
Temperature [K]	100
Detector technology	CCD
Collection date	2015-06-19
Detector	RAYONIX MX300-HS
Wavelength(s)	1.0422
Spacegroup name	P 41
Unit cell lengths	92.445, 92.445, 252.615
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	46.223 - 2.749
R-factor	0.2156
Rwork	0.214
R-free	0.26650
RMSD bond length	0.012
RMSD bond angle	1.562
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	46.223
High resolution limit [Å]	2.749
Number of reflections	54277
<I/σ(I)>	20.5
Completeness [%]	98.9
Redundancy	3.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	EVAPORATION		298	200 mM MgSO4, 20% PEG3350