5JEL

Phosphorylated TRIF in complex with IRF-3

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 5.0.1
Synchrotron site	ALS
Beamline	5.0.1
Temperature [K]	120
Detector technology	CCD
Collection date	2015-05-28
Detector	ADSC QUANTUM 315r
Wavelength(s)	1.0
Spacegroup name	P 32 2 1
Unit cell lengths	72.811, 72.811, 127.602
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	44.848 - 1.600
R-factor	0.1687
Rwork	0.168
R-free	0.18710
RMSD bond length	0.006
RMSD bond angle	1.039
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	PHASER
Refinement software	PHENIX (1.9_1692)

Data quality characteristics

	Overall
Low resolution limit [Å]	44.848
High resolution limit [Å]	1.600
Number of reflections	52282
<I/σ(I)>	45.2
Completeness [%]	99.8
Redundancy	11.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		277	0.1M NaAc pH 4.6, 2.0M NaCl