5J7U

Faustovirus major capsid protein

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 23-ID-D
Synchrotron site	APS
Beamline	23-ID-D
Temperature [K]	100
Detector technology	PIXEL
Collection date	2014-07-12
Detector	DECTRIS PILATUS 6M
Wavelength(s)	1.03318
Spacegroup name	P 1 21 1
Unit cell lengths	86.380, 390.830, 130.140
Unit cell angles	90.00, 91.66, 90.00

Refinement procedure

Resolution	72.919 - 2.440
R-factor	0.207
Rwork	0.205
R-free	0.25200
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	5j7o
RMSD bond length	0.003
RMSD bond angle	0.606
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER (2.5.6)
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	78.170	2.500
High resolution limit [Å]	2.440	2.440
Rmerge	0.230
Number of reflections	317565
<I/σ(I)>	8
Completeness [%]	99.8
Redundancy	4.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	1.6 M ammonium sulfate, 10% dioxane