5J2V

Crystal Structure of Hsp90-alpha Apo N-domain

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	200
Detector technology	PIXEL
Collection date	2015-09-15
Detector	DECTRIS PILATUS3 X 1M
Wavelength(s)	1.0
Spacegroup name	I 2 2 2
Unit cell lengths	67.765, 92.400, 103.533
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	46.200 - 1.590
Rwork	0.186
R-free	0.20300
RMSD bond length	0.014
RMSD bond angle	1.060
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	BUSTER-TNT (2.10.2)

Data quality characteristics

	Overall
Low resolution limit [Å]	46.200
High resolution limit [Å]	1.590
Number of reflections	43963
<I/σ(I)>	23.71
Completeness [%]	99.9
Redundancy	6.56

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		277.15	0.2 M sodium fluoride, 0.1 M Bis Tris propane, 20 % w/v PEG 3350