5J1K

Crystal structure of Csd2-Csd2 dimer

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 5C (4A)
Synchrotron site	PAL/PLS
Beamline	5C (4A)
Temperature [K]	100
Detector technology	CCD
Collection date	2014-11-07
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.97960
Spacegroup name	P 61 2 2
Unit cell lengths	140.772, 140.772, 40.244
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	50.010 - 1.810
R-factor	0.18249
Rwork	0.181
R-free	0.21822
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.011
RMSD bond angle	1.428
Data scaling software	HKL-2000
Phasing software	MOLREP
Refinement software	REFMAC (5.8.0123)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.010	1.830
High resolution limit [Å]	1.800	1.800
Number of reflections	22028
<I/σ(I)>	47.1	6.9
Completeness [%]	99.8	98.6
Redundancy	16.4	17

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		296	HEPES, Jeffamine ED-2001