5IMW
Trapped Toxin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-10-01 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9537 |
Spacegroup name | P 21 2 21 |
Unit cell lengths | 84.465, 101.565, 175.735 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.135 - 2.890 |
R-factor | 0.2603 |
Rwork | 0.258 |
R-free | 0.29500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1s3r |
RMSD bond length | 0.003 |
RMSD bond angle | 0.540 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 48.135 |
High resolution limit [Å] | 2.890 |
Number of reflections | 34453 |
<I/σ(I)> | 10.9 |
Completeness [%] | 98.8 |
Redundancy | 14.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | MES, NaCl, PEG 8000 |