5IK3
Crystal structure of anti-gliadin 1002-1E03 Fab fragment
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-09-12 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.07192 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 77.280, 138.810, 91.720 |
Unit cell angles | 90.00, 108.20, 90.00 |
Refinement procedure
Resolution | 69.400 - 1.650 |
R-factor | 0.1977 |
Rwork | 0.196 |
R-free | 0.23610 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5ijk |
RMSD bond length | 0.012 |
RMSD bond angle | 1.327 |
Data reduction software | xia |
Refinement software | PHENIX ((1.10.1_2155)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 69.400 | 1.690 |
High resolution limit [Å] | 1.650 | 1.650 |
Number of reflections | 109856 | |
<I/σ(I)> | 14.9 | |
Completeness [%] | 99.9 | |
Redundancy | 13.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2M Ammonium sulfate, 30% PEK 8000 |