5IIZ

Xanthomonas campestris Peroxiredoxin Q - Structure F0

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 5.0.2
Synchrotron site	ALS
Beamline	5.0.2
Temperature [K]	200
Detector technology	CCD
Collection date	2014-06-14
Detector	ADSC QUANTUM 270
Wavelength(s)	0.89014
Spacegroup name	P 1 21 1
Unit cell lengths	35.400, 51.360, 39.955
Unit cell angles	90.00, 103.27, 90.00

Refinement procedure

Resolution	34.455 - 1.050
R-factor	0.1358
Rwork	0.135
R-free	0.15340
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3gkm
RMSD bond length	0.007
RMSD bond angle	1.027
Data reduction software	iMOSFLM
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	PHENIX ((dev_2386: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	35.000
High resolution limit [Å]	1.050	1.050
Number of reflections	63833
<I/σ(I)>	11.8
Completeness [%]	98.0
Redundancy	7
CC(1/2)	0.700

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	5.5	300	30% PEG 4000, 0.1 M sodium acetate pH 5.5, 10 mM DTT