Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 21-ID-D |
| Synchrotron site | APS |
| Beamline | 21-ID-D |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-10-10 |
| Detector | MARMOSAIC 300 mm CCD |
| Wavelength(s) | 0.97910 |
| Spacegroup name | P 41 2 2 |
| Unit cell lengths | 47.714, 47.714, 193.488 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 38.300 - 1.900 |
| R-factor | 0.179 |
| Rwork | 0.175 |
| R-free | 0.21280 |
| Structure solution method | SAD |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.644 |
| Data reduction software | HKL-2000 |
| Phasing software | PHENIX (1.9_1690) |
| Refinement software | PHENIX (1.9_1690) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 38.300 | 1.950 |
| High resolution limit [Å] | 1.830 | 1.830 |
| Number of reflections | 37570 | |
| <I/σ(I)> | 22.87 | 1.13 |
| Completeness [%] | 99.8 | 98.1 |
| Redundancy | 1.81 | 1.81 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 292 | zinc acetate, sodium cacodylate, magnesium chloride, isopropanol |
