5HXY
Crystal structure of XerA recombinase
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-5A |
| Synchrotron site | Photon Factory |
| Beamline | BL-5A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2008-03-03 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.97952, 0.97987, 0.9800 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 182.860, 105.968, 115.586 |
| Unit cell angles | 90.00, 110.01, 90.00 |
Refinement procedure
| Resolution | 47.660 - 2.500 |
| R-factor | 0.19129 |
| Rwork | 0.188 |
| R-free | 0.24321 |
| Structure solution method | MAD |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.820 |
| Data scaling software | HKL-2000 |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.500 |
| Number of reflections | 68638 |
| <I/σ(I)> | 13.69 |
| Completeness [%] | 95.4 |
| Redundancy | 3.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 295.5 | PEG 4000, ADA, LiSO4 |
