5HTG

Structure of apo P1 form of Candida albicans FKBP12

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	OTHER
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2014-10-12
Detector	RIGAKU RAXIS HTC
Wavelength(s)	1.5418
Spacegroup name	P 1
Unit cell lengths	35.899, 38.643, 50.429
Unit cell angles	78.56, 69.67, 79.31

Refinement procedure

Resolution	18.000 - 2.400
R-factor	0.2205
Rwork	0.217
R-free	0.25350
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.003
RMSD bond angle	0.658
Data reduction software	MOSFLM
Data scaling software	SCALA
Phasing software	MOLREP
Refinement software	PHENIX (1.6.4_486)

Data quality characteristics

	Overall
Low resolution limit [Å]	18.000
High resolution limit [Å]	2.400
Number of reflections	18999
<I/σ(I)>	5
Completeness [%]	85.0
Redundancy	1.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		298	PEG 4000, tris