Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 HF |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2015-01-01 |
| Detector | RIGAKU RAXIS IV++ |
| Wavelength(s) | 0.97920 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 119.350, 50.650, 90.310 |
| Unit cell angles | 90.00, 129.37, 90.00 |
Refinement procedure
| Resolution | 50.000 - 1.740 |
| R-factor | 0.17266 |
| Rwork | 0.171 |
| R-free | 0.20449 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4e0r |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.048 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0071) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.790 |
| High resolution limit [Å] | 1.740 | 1.740 |
| Number of reflections | 42201 | |
| <I/σ(I)> | 17.5 | 3 |
| Completeness [%] | 98.5 | 98.3 |
| Redundancy | 3.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.2 M Sodium citrate tribasic dihydrate, 20% w/v Polyethylene glycol 3350 |
