5GZ2

luciferase complex with 7-cy-L

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 12.3.1
Synchrotron site	ALS
Beamline	12.3.1
Temperature [K]	100
Detector technology	CCD
Collection date	2016-06-20
Detector	RAYONIX MX-225
Wavelength(s)	0.9791
Spacegroup name	P 41
Unit cell lengths	74.154, 74.154, 95.622
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	40.180 - 2.000
R-factor	0.209
Rwork	0.208
R-free	0.23900
RMSD bond length	0.010
RMSD bond angle	1.123
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.990
Number of reflections	35023
<I/σ(I)>	51.3
Completeness [%]	100.0
Redundancy	7.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		290	Sodium malonate , PEG3350