5GQM

Crystal structure of in cellulo Wild Type Cypovirus Polyhedra

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL32XU
Synchrotron site	SPring-8
Beamline	BL32XU
Temperature [K]	100
Detector technology	CCD
Collection date	2016-04-25
Detector	RAYONIX MX325HE
Wavelength(s)	1
Spacegroup name	I 2 3
Unit cell lengths	103.420, 103.420, 103.420
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	42.220 - 1.680
R-factor	0.15221
Rwork	0.148
R-free	0.19550
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2oh6
RMSD bond length	0.019
RMSD bond angle	1.951
Refinement software	REFMAC (5.8.0135)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.780
High resolution limit [Å]	1.680	1.680
Number of reflections	20993
<I/σ(I)>	6.06
Completeness [%]	99.4
Redundancy	7.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	IN CELL		300	In vivo crystallization