5GL6

Msmeg rimP

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU FR-E+ SUPERBRIGHT
Temperature [K]	113
Detector technology	IMAGE PLATE
Collection date	2012-01-01
Detector	RIGAKU RAXIS IV++
Wavelength(s)	1.54187
Spacegroup name	P 21 21 21
Unit cell lengths	55.990, 75.440, 109.990
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	31.283 - 2.200
R-factor	0.2328
Rwork	0.231
R-free	0.26250
RMSD bond length	0.009
RMSD bond angle	1.239
Data reduction software	SCALA
Data scaling software	SCALA
Phasing software	CRANK
Refinement software	PHENIX (1.8_1069)

Data quality characteristics

	Overall
Low resolution limit [Å]	39.220
High resolution limit [Å]	2.200
Rmerge	0.056
Number of reflections	24283
<I/σ(I)>	14.4
Completeness [%]	100.0
Redundancy	6.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	8	289	20% PEG 3350, 6% Acetonitrile, 0.2M sodium citrate