5G45
Ligand complex of RORg LBD
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Detector | PILATUS |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 62.220, 62.220, 154.060 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 21.000 - 2.070 |
| R-factor | 0.2106 |
| Rwork | 0.208 |
| R-free | 0.25550 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.010 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Refinement software | BUSTER (2.11.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 21.000 | 2.140 |
| High resolution limit [Å] | 2.070 | 2.070 |
| Rmerge | 0.260 | 1.500 |
| Number of reflections | 19313 | |
| <I/σ(I)> | 10.2 | 1.8 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 12.4 | 13.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
