5FWV

Wnt modulator Kremen crystal form III at 3.2A

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04
Synchrotron site	Diamond
Beamline	I04
Temperature [K]	100
Detector technology	PIXEL
Collection date	2013-09-15
Detector	DECTRIS PILATUS
Spacegroup name	P 41 21 2
Unit cell lengths	67.844, 67.844, 198.193
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	64.190 - 3.200
R-factor	0.1988
Rwork	0.195
R-free	0.26484
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.016
RMSD bond angle	1.872
Data reduction software	XDS
Data scaling software	Aimless
Refinement software	REFMAC (5.8.0135)

Data quality characteristics

	Overall
Low resolution limit [Å]	67.800
High resolution limit [Å]	3.200
Rmerge	0.300
Number of reflections	8171
<I/σ(I)>	13.1
Completeness [%]	98.8
Redundancy	22.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		7.5		0.1 M HEPES/MOPS 7.5 30 % P550MME_P20K DRIED OUT