5FWB

Human Spectrin SH3 domain D48G, E7F, K60F

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALBA BEAMLINE XALOC
Synchrotron site	ALBA
Beamline	XALOC
Temperature [K]	100
Detector technology	PIXEL
Detector	DECTRIS PILATUS 6M
Spacegroup name	P 21 21 21
Unit cell lengths	33.868, 38.816, 42.422
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	28.640 - 1.500
R-factor	0.20737
Rwork	0.206
R-free	0.23562
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.027
RMSD bond angle	2.350
Refinement software	REFMAC (5.5.0109)

Data quality characteristics

	Overall
Low resolution limit [Å]	38.820
High resolution limit [Å]	1.500
Rmerge	0.110
Number of reflections	9427
<I/σ(I)>	8.7
Completeness [%]	99.5
Redundancy	5.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1