5FTP
sulfur SAD phasing of Cdc23Nterm: data collection with a tailored X- ray beam size at 2.69 A wavelength (4.6 keV)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P13 (MX1) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P13 (MX1) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-07-10 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 43 |
Unit cell lengths | 61.249, 61.249, 151.559 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 61.250 - 3.100 |
R-factor | 0.19046 |
Rwork | 0.187 |
R-free | 0.25963 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.009 |
RMSD bond angle | 1.397 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | SHELXD |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 61.250 | 3.210 |
High resolution limit [Å] | 3.100 | 3.100 |
Rmerge | 0.110 | 0.720 |
Number of reflections | 282255 | |
<I/σ(I)> | 30.1 | 4.8 |
Completeness [%] | 99.7 | 98 |
Redundancy | 27.8 | 17.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | CRYSTALLIZATION DETAILS AS PER 3ZN3 |