5FQ0
The structure of KdgF from Halomonas sp.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 113 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 110.934, 78.680, 68.002 |
| Unit cell angles | 90.00, 113.91, 90.00 |
Refinement procedure
| Resolution | 62.360 - 2.000 |
| R-factor | 0.18682 |
| Rwork | 0.185 |
| R-free | 0.22448 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 5fpx |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.777 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 60.000 | 2.410 |
| High resolution limit [Å] | 2.350 | 2.350 |
| Rmerge | 0.100 | 0.400 |
| Number of reflections | 22373 | |
| <I/σ(I)> | 6.8 | 2.1 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 3.7 | 3.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
