5FPX

The structure of KdgF from Yersinia enterocolitica.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CLSI BEAMLINE 08ID-1
Synchrotron site	CLSI
Beamline	08ID-1
Temperature [K]	113
Detector technology	CCD
Detector	MARRESEARCH
Spacegroup name	P 21 21 21
Unit cell lengths	39.920, 73.760, 83.680
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	55.330 - 1.500
R-factor	0.17264
Rwork	0.171
R-free	0.19928
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2pfw
RMSD bond length	0.015
RMSD bond angle	1.827
Data reduction software	XDS
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	REFMAC (5.8.0073)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000	1.530
High resolution limit [Å]	1.500	1.500
Rmerge	0.030	0.440
Number of reflections	39140
<I/σ(I)>	32.2	3.6
Completeness [%]	97.3	78.5
Redundancy	7.2	6.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1