5FPA
Crystal structure of human KDM4D in complex with 3H,4H-pyrido-3,4-d- pyrimidin-4-one
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-12-08 |
Detector | RIGAKU SATURN A200 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 71.525, 71.525, 150.366 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 64.590 - 1.960 |
R-factor | 0.17096 |
Rwork | 0.169 |
R-free | 0.21060 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | NONE |
RMSD bond length | 0.006 |
RMSD bond angle | 1.017 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.990 |
High resolution limit [Å] | 1.960 | 1.960 |
Rmerge | 0.100 | 0.100 |
Number of reflections | 28865 | |
<I/σ(I)> | 2 | 5.2 |
Completeness [%] | 99.8 | 100 |
Redundancy | 5.1 | 5.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.4 | 0.1M HEPES, PH 7.4, 2.2M AMSO4 |