5FIH
SACCHAROMYCES CEREVISIAE GAS2P (E176Q MUTANT) IN COMPLEX WITH LAMINARITETRAOSE AND LAMINARIPENTAOSE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF |
Synchrotron site | ESRF |
Temperature [K] | 100 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 50.115, 70.258, 149.916 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.800 |
R-factor | 0.21701 |
Rwork | 0.217 |
R-free | 0.24439 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2w61 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.332 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.070 | 0.430 |
Number of reflections | 49626 | |
<I/σ(I)> | 30 | 3.1 |
Completeness [%] | 98.3 | 97.3 |
Redundancy | 4.1 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |