5FBY

Crystal structure of ctSPD

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 8.2.1
Synchrotron site	ALS
Beamline	8.2.1
Temperature [K]	100
Detector technology	CCD
Collection date	2015-01-27
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.979
Spacegroup name	P 21 21 21
Unit cell lengths	55.559, 98.889, 107.747
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	49.381 - 1.898
R-factor	0.1721
Rwork	0.171
R-free	0.19800
RMSD bond length	0.011
RMSD bond angle	1.262
Phasing software	HKL-3000
Refinement software	PHENIX (dev_1839)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.898
Number of reflections	47718
<I/σ(I)>	27.7
Completeness [%]	100.0
Redundancy	7.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	PEG3350, ammonium citrate tribasic