5F88
Cetuximab Fab in complex with L5Y meditope variant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2011-04-18 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 64.240, 83.140, 211.940 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.706 - 2.481 |
R-factor | 0.1653 |
Rwork | 0.163 |
R-free | 0.21650 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4gw1 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.664 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | PHENIX ((1.10_2155)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 33.150 | 2.550 |
High resolution limit [Å] | 2.480 | 2.480 |
Number of reflections | 39080 | |
<I/σ(I)> | 25.2 | 9.2 |
Completeness [%] | 95.1 | 72.3 |
Redundancy | 5.2 | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M citrate, 0.1 M Na2HPO4, 0.5 M K2HPO4, 1.6 M NaH2PO4 |