5F0U
Crystal structure of Gold binding protein
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU FR-E+ SUPERBRIGHT |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2014-07-18 |
| Detector | RIGAKU RAXIS IV++ |
| Wavelength(s) | 1.5419 |
| Spacegroup name | P 65 2 2 |
| Unit cell lengths | 37.095, 37.095, 170.032 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 32.130 - 1.680 |
| R-factor | 0.19884 |
| Rwork | 0.197 |
| R-free | 0.22699 |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.582 |
| Data reduction software | HKL-3000 |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.710 |
| High resolution limit [Å] | 1.680 | 1.680 |
| Number of reflections | 8466 | |
| <I/σ(I)> | 24.31 | 3.756 |
| Completeness [%] | 98.0 | |
| Redundancy | 11.6 | 2.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 2.0 M Ammonium citrate tribasic, 0.1 M BIS-TRIS propane |
