5EWP

ARO (armadillo repeats only protein) from Plasmodium falciparum

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CLSI BEAMLINE 08ID-1
Synchrotron site	CLSI
Beamline	08ID-1
Temperature [K]	100
Detector technology	CCD
Collection date	2015-08-15
Detector	MARMOSAIC 300 mm CCD
Wavelength(s)	0.9798
Spacegroup name	P 1
Unit cell lengths	46.800, 54.940, 64.650
Unit cell angles	106.68, 100.57, 99.60

Refinement procedure

Resolution	33.856 - 1.800
R-factor	0.1704
Rwork	0.169
R-free	0.19170
Structure solution method	SAD
RMSD bond length	0.007
RMSD bond angle	1.033
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX (1.9_1692)

Data quality characteristics

	Overall
Low resolution limit [Å]	47.360
High resolution limit [Å]	1.800
Number of reflections	96059
<I/σ(I)>	7.9
Completeness [%]	97.1
Redundancy	1.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	0.2M potassium flouride, 20% PEG3350