5EQW
Structure of the major structural protein D135 of Acidianus tailed spindle virus (ATSV)
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL9-1 |
| Synchrotron site | SSRL |
| Beamline | BL9-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-01-19 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.95369 |
| Spacegroup name | P 1 2 1 |
| Unit cell lengths | 97.780, 41.672, 97.690 |
| Unit cell angles | 90.00, 108.64, 90.00 |
Refinement procedure
| Resolution | 38.005 - 1.679 |
| R-factor | 0.1904 |
| Rwork | 0.189 |
| R-free | 0.21600 |
| Structure solution method | MAD |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.003 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 1.679 |
| Number of reflections | 84697 |
| <I/σ(I)> | 16.26 |
| Completeness [%] | 98.7 |
| Redundancy | 3.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 2.6 | 295 | Sodium nitrate, sodium acetate, glycerol, acetonitrile |
