5EO1

Crystal Structure of HLA-B0702-RL9

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	AUSTRALIAN SYNCHROTRON BEAMLINE MX2
Synchrotron site	Australian Synchrotron
Beamline	MX2
Temperature [K]	100
Detector technology	CCD
Collection date	2014-09-29
Detector	ADSC QUANTUM 315r
Wavelength(s)	.987
Spacegroup name	P 21 21 21
Unit cell lengths	50.662, 81.857, 110.366
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	46.040 - 1.850
R-factor	0.204
Rwork	0.201
R-free	0.25850
RMSD bond length	0.002
RMSD bond angle	0.507
Data reduction software	iMOSFLM
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	PHENIX (1.9_1692)

Data quality characteristics

	Overall
Low resolution limit [Å]	46.040
High resolution limit [Å]	1.850
Number of reflections	39928
<I/σ(I)>	9.8
Completeness [%]	99.8
Redundancy	7.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	PEG4K, Ammonium acetate, Na-cacodylate