5EKZ

Crystal structure of mouse Taco1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE MASSIF-3
Synchrotron site	ESRF
Beamline	MASSIF-3
Temperature [K]	294
Detector technology	CCD
Collection date	2015-06-18
Detector	MARMOSAIC 225 mm CCD
Wavelength(s)	0.9677
Spacegroup name	P 21 21 21
Unit cell lengths	48.550, 55.380, 92.050
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.468 - 2.000
R-factor	0.2032
Rwork	0.202
R-free	0.22090
RMSD bond length	0.013
RMSD bond angle	1.062
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	AutoSol
Refinement software	PHENIX

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	100.000		2.070
High resolution limit [Å]	2.000	4.310	2.000
Rmerge	0.056	0.029	1.106
Rmeas	0.061	0.032	1.203
Total number of observations	108871
Number of reflections	17352	1861	1657
<I/σ(I)>	17.41	46.78	1.73
Completeness [%]	99.9	99.8	99.8
Redundancy	6.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		298	200 mM Ammonium Nitrate, 160 mM Sodium Thiocyanate, 10 % Peg 400, and 20 % Peg 3350