5EJ3
Crystal structure of XlnB2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 21-ID-D |
| Synchrotron site | APS |
| Beamline | 21-ID-D |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2012-05-10 |
| Detector | MARMOSAIC 300 mm CCD |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 41.097, 66.941, 65.483 |
| Unit cell angles | 90.00, 94.11, 90.00 |
Refinement procedure
| Resolution | 46.749 - 1.314 |
| R-factor | 0.1313 |
| Rwork | 0.130 |
| R-free | 0.16680 |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.423 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 46.749 |
| High resolution limit [Å] | 1.310 |
| Number of reflections | 81872 |
| <I/σ(I)> | 12.2 |
| Completeness [%] | 96.4 |
| Redundancy | 4.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2 M zinc acetate dehydrate, 0.1 M sodium acetate pH 4.5 and 10 % w/v PEG 3000 |
