5ECM
Crystal Structure of FIN219-FIP1 complex with JA and Leu
Experimental procedure
Experimental method | LAUE |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE BL13C1 |
Synchrotron site | NSRRC |
Beamline | BL13C1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-11-08 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 0.9762-0.97622 |
Spacegroup name | P 1 |
Unit cell lengths | 53.822, 53.901, 195.815 |
Unit cell angles | 97.15, 92.27, 113.64 |
Refinement procedure
Resolution | 24.168 - 1.600 |
R-factor | 0.2331 |
Rwork | 0.232 |
R-free | 0.24550 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4epl |
RMSD bond length | 0.009 |
RMSD bond angle | 1.548 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER (2.5.6) |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.660 |
High resolution limit [Å] | 1.600 | 3.450 | 1.600 |
Rmerge | 0.083 | 0.062 | 0.518 |
Total number of observations | 579160 | ||
Number of reflections | 259707 | ||
<I/σ(I)> | 6.1 | ||
Completeness [%] | 95.0 | 89.8 | 95.1 |
Redundancy | 2.3 | 2.3 | 2.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 297 | 0.2 M sodium acetate trihydrate, 0.1 M Tris-HCl, 30%(w/v) PEG 3000 |