5E1P
Ca(2+)-Calmodulin from Paramecium tetraurelia qFit disorder model
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 1999-07-21 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.886 |
Spacegroup name | P 1 |
Unit cell lengths | 25.015, 29.415, 52.761 |
Unit cell angles | 89.54, 86.10, 82.39 |
Refinement procedure
Resolution | 25.520 - 1.010 |
R-factor | 0.127 |
Rwork | 0.125 |
R-free | 0.14200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1exr |
RMSD bond length | 0.010 |
RMSD bond angle | 1.317 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.520 | 1.040 |
High resolution limit [Å] | 1.000 | 1.000 |
Rmerge | 0.073 | 0.506 |
Number of reflections | 78247 | |
<I/σ(I)> | 17.4 | 2.1 |
Completeness [%] | 96.9 | 83.9 |
Redundancy | 5.4 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 277 | 50 mM sodium cacodylate, 50% MPD |