5DVB
Crystal Structure of S. cerevisiae TSA2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-02-15 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.9786 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 171.530, 216.130, 64.490 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.716 - 2.200 |
R-factor | 0.1877 |
Rwork | 0.187 |
R-free | 0.23270 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3sbc |
RMSD bond length | 0.015 |
RMSD bond angle | 1.435 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.10_2152: ???)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 42.880 | 2.250 | |
High resolution limit [Å] | 2.200 | 40.000 | 2.200 |
Rmerge | 0.166 | 0.854 | 4.961 |
Rmeas | 0.166 | 0.891 | 4.994 |
Total number of observations | 15148713 | ||
Number of reflections | 122589 | 13 | 7902 |
<I/σ(I)> | 33.67 | 5.64 | 1.11 |
Completeness [%] | 100.0 | 39.4 | 100 |
Redundancy | 124 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 293 | 6% (v/v) Tacsimate pH 8 and 16% (w/v) PEG3350 |