5DIP

Crystal structure of lpg0406 in reduced form from Legionella pneumophila

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U
Synchrotron site	SSRF
Beamline	BL17U
Temperature [K]	100
Detector technology	CCD
Collection date	2015-07-05
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.97861
Spacegroup name	I 21 3
Unit cell lengths	145.712, 145.712, 145.712
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	28.576 - 2.097
R-factor	0.1354
Rwork	0.134
R-free	0.15800
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	5dik
RMSD bond length	0.007
RMSD bond angle	1.123
Refinement software	PHENIX (1.8.4_1496)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.097
Number of reflections	30286
<I/σ(I)>	29.1
Completeness [%]	100.0
Redundancy	20

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	4.5	287	0.1 M sodium acetate, 22% PEG 3350