5D74

The crystal structure of Ly7917

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2014-12-03
Detector	PSI PILATUS 6M
Wavelength(s)	0.97852
Spacegroup name	C 2 2 21
Unit cell lengths	70.009, 97.701, 174.668
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	34.643 - 1.900
R-factor	0.1977
Rwork	0.196
R-free	0.23370
Structure solution method	SAD
RMSD bond length	0.007
RMSD bond angle	1.011
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Phasing software	SHELXDE
Refinement software	PHENIX (1.9_1692)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.970
High resolution limit [Å]	1.900	1.900
Number of reflections	47363
<I/σ(I)>	15.9
Completeness [%]	99.8
Redundancy	13.1	11.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7	291	0.1M Tris, 0.8M LiCl